TA Instruments

AR1771-0002f

28/03/2013 11:51:36

Sample name	DI 40 mm AL P240B 10 mm gap
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	mr1
Sample density	1.000 g/cm^3
Results file name	AR1771
Run number	2 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	28/03/2013 11:51:36

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	40 mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	40.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	2.000 
Shear stress factor	79580 1/m^3
Measurement system factor	39790 1/m^3
Fluid density factor	8.378E-10 m^5
Normal force factor	1592 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	12.57 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	4.461	-45.108	10000	20.0	5.863	31.004	-3.590	8.922	-0.4023	9332	1.9060	117.2	3.8120	381.20	3.411E-3	0.0	0.5
2.0040	9.997	12.946	10000	20.0	5.864	32.004	1.030	19.99	0.05152	9333	13.3236	23.35	26.647	2664.7	3.411E-3	0.0	0.5
3.0200	15.50	24.056	10000	20.0	5.864	33.020	1.914	30.99	0.06176	9332	26.9225	9.715	53.845	5384.5	3.411E-3	0.1	0.6
4.0040	18.44	31.076	10000	20.0	5.860	34.004	2.473	36.87	0.06707	9327	40.9615	6.859	81.923	8192.3	3.411E-3	0.1	0.6
5.0200	24.68	48.092	10000	20.0	5.862	35.020	3.827	49.36	0.07754	9330	67.6173	3.830	135.23	13523	3.411E-3	0.1	0.6
6.0200	31.59	69.903	10000	20.0	5.859	36.020	5.563	63.18	0.08804	9324	106.6750	2.336	213.35	21335	3.411E-3	0.1	0.6
7.0200	34.03	78.008	10000	20.0	5.857	37.020	6.208	68.06	0.09120	9322	126.3410	2.012	252.68	25268	3.411E-3	0.1	0.6
8.0200	39.31	97.574	10000	20.0	5.852	38.020	7.765	78.61	0.09877	9313	165.2590	1.507	330.52	33052	3.411E-3	0.1	0.6
9.0240	46.03	125.84	10000	20.0	5.849	39.024	10.01	92.06	0.1088	9310	223.1360	1.098	446.27	44627	3.411E-3	0.2	0.7
10.020	50.95	148.33	10000	20.0	5.845	40.020	11.80	101.9	0.1158	9303	274.6920	0.8958	549.38	54938	3.411E-3	0.2	0.7
11.000	55.72	171.14	10000	20.0	5.843	41.000	13.62	111.4	0.1222	9300	326.0270	0.7489	652.05	65205	3.411E-3	0.2	0.7
12.016	60.10	194.25	10000	20.0	5.837	42.016	15.46	120.2	0.1286	9290	377.1700	0.6430	754.34	75434	3.411E-3	0.2	0.7
13.016	64.41	216.23	10000	20.0	5.837	43.016	17.21	128.8	0.1336	9289	434.7500	0.5598	869.50	86950	3.411E-3	0.2	0.7
14.004	69.15	244.20	10000	20.0	5.830	44.004	19.43	138.3	0.1405	9279	498.6210	0.4852	997.24	99724	3.411E-3	0.2	0.7
15.020	75.68	279.62	10000	20.0	5.823	45.020	22.25	151.4	0.1470	9268	594.1520	0.4045	1188.3	1.1883E5	3.411E-3	0.3	0.8
16.016	79.93	306.20	10000	20.0	5.818	46.016	24.37	159.9	0.1524	9260	664.2600	0.3624	1328.5	1.3285E5	3.411E-3	0.3	0.8
17.016	84.53	333.92	10000	20.0	5.814	47.016	26.57	169.1	0.1572	9254	740.6160	0.3238	1481.2	1.4812E5	3.411E-3	0.3	0.8
18.020	90.98	378.40	10000	20.0	5.801	48.020	30.11	182.0	0.1655	9232	855.4930	0.2788	1711.0	1.7110E5	3.411E-3	0.3	0.8
19.004	95.04	400.91	10000	20.0	5.796	49.004	31.90	190.1	0.1678	9225	931.1690	0.2553	1862.3	1.8623E5	3.411E-3	0.3	0.8
20.012	99.40	432.92	10000	20.0	5.789	50.012	34.45	198.8	0.1733	9214	1020.8800	0.2332	2041.8	2.0418E5	3.411E-3	0.3	0.8
21.016	105.8	478.05	10000	20.0	5.776	51.016	38.04	211.7	0.1797	9193	1153.3101	0.2052	2306.6	2.3066E5	3.411E-3	0.4	0.9
22.016	109.9	513.01	10000	20.0	5.771	52.016	40.82	219.8	0.1857	9186	1242.7800	0.1902	2485.6	2.4856E5	3.411E-3	0.4	0.9
23.016	114.2	540.57	10000	20.0	5.766	53.016	43.02	228.5	0.1883	9177	1343.3800	0.1758	2686.8	2.6868E5	3.411E-3	0.4	0.9
24.024	120.6	591.64	10000	20.0	5.757	54.024	47.08	241.3	0.1951	9163	1495.5300	0.1574	2991.1	2.9911E5	3.411E-3	0.4	0.9
25.004	124.7	622.00	10000	20.0	5.749	55.004	49.50	249.5	0.1984	9149	1597.4900	0.1470	3195.0	3.1950E5	3.411E-3	0.4	0.9
26.020	129.1	654.07	10000	20.0	5.744	56.020	52.05	258.1	0.2017	9142	1711.6300	0.1372	3423.3	3.4233E5	3.411E-3	0.4	0.9
27.016	135.4	712.32	10000	20.0	5.729	57.016	56.68	270.9	0.2093	9119	1881.8400	0.1243	3763.7	3.7637E5	3.411E-3	0.5	1.0
28.000	139.5	749.93	10000	20.0	5.726	58.000	59.68	279.1	0.2138	9113	1995.6100	0.1170	3991.2	3.9912E5	3.411E-3	0.5	1.0
29.024	143.6	779.74	10000	20.0	5.713	59.024	62.05	287.3	0.2160	9093	2116.5400	0.1102	4233.1	4.2331E5	3.411E-3	0.5	1.0
30.016	150.0	836.83	10000	20.0	5.704	60.016	66.59	300.1	0.2219	9078	2305.6201	0.1008	4611.2	4.6112E5	3.411E-3	0.5	1.0
31.020	154.1	873.60	10000	20.0	5.701	61.020	69.52	308.3	0.2255	9073	2431.9800	0.09546	4864.0	4.8640E5	3.411E-3	0.5	1.0
32.004	158.2	917.97	10000	20.0	5.689	62.004	73.05	316.5	0.2308	9054	2635.4600	0.09039	5270.9	5.2709E5	3.411E-3	0.5	1.0
33.016	164.7	980.23	10000	20.0	5.677	63.016	78.00	329.3	0.2369	9035	2774.0901	0.08332	5548.2	5.5482E5	3.411E-3	0.6	1.1
34.024	168.8	1029.5	10000	20.0	5.666	64.024	81.93	337.5	0.2427	9017	2912.3899	0.07915	5824.8	5.8248E5	3.411E-3	0.6	1.1
35.004	174.9	1084.3	10000	20.0	5.653	65.004	86.29	349.7	0.2467	8997	3127.2900	0.07356	6254.6	6.2546E5	3.411E-3	0.6	1.1
36.016	179.1	1120.3	10000	20.0	5.641	66.016	89.15	358.2	0.2489	8977	3282.2300	0.06995	6564.5	6.5645E5	3.411E-3	0.6	1.1
37.016	183.3	1166.1	10000	20.0	5.628	67.016	92.80	366.5	0.2532	8957	3506.9700	0.06668	7013.9	7.0139E5	3.411E-3	0.6	1.1
38.016	189.3	1230.6	10000	20.0	5.618	68.016	97.92	378.6	0.2586	8942	3657.8000	0.06238	7315.6	7.3156E5	3.411E-3	0.6	1.1
39.024	193.5	1276.2	10000	20.0	5.613	69.024	101.6	386.9	0.2625	8933	3822.0500	0.05967	7644.1	7.6441E5	3.411E-3	0.7	1.2
40.016	199.7	1347.3	10000	20.0	5.588	70.016	107.2	399.3	0.2685	8894	4068.3101	0.05577	8136.6	8.1366E5	3.411E-3	0.7	1.2
41.012	203.7	1387.9	10000	20.0	5.582	71.012	110.4	407.4	0.2711	8885	4232.3999	0.05353	8464.8	8.4648E5	3.411E-3	0.7	1.2
42.016	210.0	1464.7	10000	20.0	5.557	72.016	116.6	419.9	0.2776	8845	4498.5298	0.05016	8997.1	8.9971E5	3.411E-3	0.7	1.2
43.016	214.1	1517.5	10000	20.0	5.544	73.016	120.8	428.2	0.2821	8823	4674.3599	0.04813	9348.7	9.3487E5	3.411E-3	0.7	1.2
44.024	218.1	1576.3	10000	20.0	5.538	74.024	125.4	436.2	0.2876	8814	4851.0298	0.04632	9702.1	9.7021E5	3.411E-3	0.7	1.2
45.000	224.3	1635.1	10000	20.0	5.521	75.000	130.1	448.5	0.2901	8787	5129.5498	0.04368	10259	1.0259E6	3.411E-3	0.8	1.3
46.012	228.4	1690.3	10000	20.0	5.504	76.012	134.5	456.8	0.2945	8760	5320.2798	0.04198	10641	1.0641E6	3.411E-3	0.8	1.3
47.016	234.5	1755.9	10000	20.0	5.494	77.016	139.7	469.0	0.2980	8744	5601.7300	0.03976	11203	1.1203E6	3.411E-3	0.8	1.3
48.016	238.5	1823.6	10000	20.0	5.473	78.016	145.1	477.0	0.3042	8710	5798.2002	0.03828	11596	1.1596E6	3.411E-3	0.8	1.3
49.028	242.7	1876.7	10000	20.0	5.454	79.028	149.3	485.3	0.3077	8680	6101.8999	0.03685	12204	1.2204E6	3.411E-3	0.8	1.3
50.016	248.7	1946.9	10000	20.0	5.456	80.016	154.9	497.5	0.3114	8683	6301.7700	0.03508	12604	1.2604E6	3.411E-3	0.8	1.3
51.016	252.8	2020.3	10000	20.0	5.446	81.016	160.8	505.6	0.3180	8668	6515.8501	0.03391	13032	1.3032E6	3.411E-3	0.9	1.4
52.016	259.0	2096.2	10000	20.0	5.408	82.016	166.8	518.1	0.3220	8607	6831.4902	0.03207	13663	1.3663E6	3.411E-3	0.9	1.4
53.000	263.1	2153.9	10000	20.0	5.375	83.000	171.4	526.2	0.3257	8555	7046.7998	0.03090	14094	1.4094E6	3.411E-3	0.9	1.4
54.032	269.1	2259.1	10000	20.0	5.369	84.032	179.8	538.2	0.3340	8545	7373.7402	0.02950	14747	1.4747E6	3.411E-3	0.9	1.4
54.996	273.3	2343.2	10000	20.0	5.343	84.996	186.5	546.6	0.3412	8504	7600.9302	0.02847	15202	1.5202E6	3.411E-3	0.9	1.4
56.004	277.3	2427.0	10000	20.0	5.325	86.004	193.1	554.7	0.3482	8476	7828.0298	0.02755	15656	1.5656E6	3.411E-3	0.9	1.4
57.016	283.3	2562.3	10000	20.0	5.294	87.016	203.9	566.7	0.3598	8426	8168.1602	0.02624	16336	1.6336E6	3.411E-3	1.0	1.5
58.016	287.5	2648.6	10000	20.0	5.268	88.016	210.8	574.9	0.3666	8384	8407.8398	0.02536	16816	1.6816E6	3.411E-3	1.0	1.5
59.024	293.6	2778.0	10000	20.0	5.221	89.024	221.1	587.1	0.3765	8309	8767.0098	0.02411	17534	1.7534E6	3.411E-3	1.0	1.5
60.012	297.6	2903.4	10000	20.0	5.184	90.012	231.0	595.1	0.3882	8251	9006.6797	0.02330	18013	1.8013E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0080	300.0	2963.1	10000	20.0	5.141	92.008	235.8	600.0	0.3930	8182	279.5750	0.02273	559.15	55915	3.411E-3	0.0	1.5
2.0000	300.0	2951.1	10000	20.0	5.173	93.000	234.8	600.0	0.3914	8234	532.5830	0.02287	1065.2	1.0652E5	3.411E-3	0.0	1.6
3.0000	300.0	2966.9	10000	20.0	5.157	94.000	236.1	600.0	0.3935	8208	907.8180	0.02280	1815.6	1.8156E5	3.411E-3	0.1	1.6
4.0000	300.0	2968.7	10000	20.0	5.154	95.000	236.2	600.0	0.3937	8203	1159.3000	0.02279	2318.6	2.3186E5	3.411E-3	0.1	1.6
5.0000	300.0	2933.6	10000	20.0	5.154	96.000	233.4	600.0	0.3891	8202	1410.5900	0.02278	2821.2	2.8212E5	3.411E-3	0.1	1.6
6.0080	300.0	2934.5	10000	20.0	5.155	97.008	233.5	600.0	0.3892	8205	1789.0000	0.02279	3578.0	3.5780E5	3.411E-3	0.1	1.6
7.0000	300.0	2951.6	10000	20.0	5.152	98.000	234.9	600.0	0.3915	8199	2040.9600	0.02277	4081.9	4.0819E5	3.411E-3	0.1	1.6
8.0040	300.0	2939.7	10000	20.0	5.168	99.004	233.9	600.0	0.3899	8225	2417.2700	0.02284	4834.5	4.8345E5	3.411E-3	0.1	1.7
9.0080	300.0	2904.5	10000	20.0	5.178	100.008	231.1	600.0	0.3852	8241	2667.2100	0.02289	5334.4	5.3344E5	3.411E-3	0.2	1.7
10.004	300.0	2897.0	10000	20.0	5.166	101.004	230.5	600.0	0.3842	8222	2918.5200	0.02284	5837.0	5.8370E5	3.411E-3	0.2	1.7
11.008	300.0	2953.9	10000	20.0	5.181	102.008	235.1	600.0	0.3918	8246	3295.4900	0.02291	6591.0	6.5910E5	3.411E-3	0.2	1.7
12.016	300.0	2914.1	10000	20.0	5.151	103.016	231.9	600.0	0.3865	8198	3546.8301	0.02277	7093.7	7.0937E5	3.411E-3	0.2	1.7
13.008	300.0	2949.7	10000	20.0	5.164	104.008	234.7	600.0	0.3912	8219	3798.6399	0.02283	7597.3	7.5973E5	3.411E-3	0.2	1.7
14.004	300.0	2921.6	10000	20.0	5.171	105.004	232.5	600.0	0.3875	8230	4175.1401	0.02286	8350.3	8.3503E5	3.411E-3	0.2	1.8
15.016	300.0	2932.3	10000	20.0	5.143	106.016	233.3	600.0	0.3889	8186	4430.0400	0.02274	8860.1	8.8601E5	3.411E-3	0.3	1.8
16.016	300.0	2978.0	10000	20.0	5.147	107.016	237.0	600.0	0.3949	8192	4805.0200	0.02275	9610.0	9.6100E5	3.411E-3	0.3	1.8
17.000	300.0	2957.2	10000	20.0	5.160	108.000	235.3	600.0	0.3922	8212	5054.9600	0.02281	10110	1.0110E6	3.411E-3	0.3	1.8
18.000	300.0	2956.9	10000	20.0	5.165	109.000	235.3	600.1	0.3921	8220	5310.0200	0.02283	10620	1.0620E6	3.411E-3	0.3	1.8
19.000	300.0	2963.5	10000	20.0	5.155	110.000	235.8	600.0	0.3931	8205	5684.8901	0.02279	11370	1.1370E6	3.411E-3	0.3	1.8
20.004	300.0	2929.3	10000	20.0	5.167	111.004	233.1	600.1	0.3885	8224	5938.0801	0.02284	11876	1.1876E6	3.411E-3	0.3	1.9
21.004	300.0	2919.4	10000	20.0	5.169	112.004	232.3	600.0	0.3872	8227	6311.4800	0.02285	12623	1.2623E6	3.411E-3	0.4	1.9
22.000	300.0	2937.1	10000	20.0	5.146	113.000	233.7	600.1	0.3895	8190	6562.7100	0.02275	13125	1.3125E6	3.411E-3	0.4	1.9
23.000	300.0	2947.6	10000	20.0	5.174	114.000	234.6	599.9	0.3910	8235	6814.1499	0.02288	13628	1.3628E6	3.411E-3	0.4	1.9
24.000	300.0	2966.3	10000	20.0	5.156	115.000	236.0	600.0	0.3934	8206	7191.1201	0.02280	14382	1.4382E6	3.411E-3	0.4	1.9
25.000	300.0	2954.0	10000	20.0	5.151	116.000	235.1	600.0	0.3918	8197	7444.4600	0.02277	14889	1.4889E6	3.411E-3	0.4	1.9
26.008	300.0	2953.9	10000	20.0	5.148	117.008	235.1	600.0	0.3918	8193	7820.9199	0.02276	15642	1.5642E6	3.411E-3	0.4	2.0
27.000	300.0	2950.9	10000	20.0	5.172	118.000	234.8	600.0	0.3914	8232	8070.7002	0.02286	16141	1.6141E6	3.411E-3	0.5	2.0
28.000	300.0	2939.1	10000	20.0	5.171	119.000	233.9	600.1	0.3898	8230	8322.2500	0.02286	16645	1.6645E6	3.411E-3	0.5	2.0
29.000	300.0	2944.2	10000	20.0	5.151	120.000	234.3	600.0	0.3905	8198	8698.9902	0.02277	17398	1.7398E6	3.411E-3	0.5	2.0
30.000	300.0	2982.5	10000	20.0	5.155	121.000	237.3	600.0	0.3956	8204	8950.4102	0.02279	17901	1.7901E6	3.411E-3	0.5	2.0
31.008	300.0	2992.4	10000	20.0	5.165	122.008	238.1	600.0	0.3969	8221	9201.7900	0.02284	18404	1.8404E6	3.411E-3	0.5	2.0
32.000	300.0	2993.9	10000	20.0	5.171	123.000	238.2	599.9	0.3971	8229	9581.0303	0.02286	19162	1.9162E6	3.411E-3	0.5	2.1
33.012	300.0	2963.9	10000	20.0	5.123	124.012	235.9	600.0	0.3931	8154	9831.8799	0.02265	19664	1.9664E6	3.411E-3	0.6	2.1
34.000	300.0	2985.1	10000	20.0	5.187	125.000	237.5	600.0	0.3959	8255	10207.000	0.02293	20414	2.0414E6	3.411E-3	0.6	2.1
35.000	300.0	2936.8	10000	20.0	5.155	126.000	233.7	600.0	0.3895	8204	10458.300	0.02279	20917	2.0917E6	3.411E-3	0.6	2.1
36.008	300.0	2990.2	10000	20.0	5.160	127.008	238.0	600.0	0.3966	8212	10710.100	0.02281	21420	2.1420E6	3.411E-3	0.6	2.1
37.000	300.0	2977.9	10000	20.0	5.170	128.000	237.0	600.0	0.3950	8228	11088.300	0.02286	22177	2.2177E6	3.411E-3	0.6	2.1
38.000	300.0	2961.3	10000	20.0	5.185	129.000	235.7	600.0	0.3927	8253	11340.000	0.02292	22680	2.2680E6	3.411E-3	0.6	2.2
39.008	300.0	2995.9	10000	20.0	5.174	130.008	238.4	600.0	0.3974	8235	11718.800	0.02288	23438	2.3438E6	3.411E-3	0.7	2.2
40.000	300.0	2919.0	10000	20.0	5.176	131.000	232.3	600.0	0.3871	8237	11966.300	0.02288	23933	2.3933E6	3.411E-3	0.7	2.2
41.008	300.0	2959.3	10000	20.0	5.162	132.008	235.5	600.0	0.3925	8216	12217.700	0.02282	24435	2.4435E6	3.411E-3	0.7	2.2
42.000	300.0	2924.6	10000	20.0	5.168	133.000	232.7	600.0	0.3879	8225	12594.800	0.02284	25190	2.5190E6	3.411E-3	0.7	2.2
43.016	300.0	2996.4	10000	20.0	5.144	134.016	238.4	600.0	0.3974	8187	12847.300	0.02274	25695	2.5695E6	3.411E-3	0.7	2.2
43.996	300.0	2998.0	10000	20.0	5.168	134.996	238.6	600.0	0.3976	8225	13226.000	0.02285	26452	2.6452E6	3.411E-3	0.7	2.2
45.000	300.0	2933.3	10000	20.0	5.175	136.000	233.4	600.0	0.3890	8237	13474.200	0.02288	26948	2.6948E6	3.411E-3	0.8	2.3
46.008	300.0	2960.6	10000	20.0	5.155	137.008	235.6	600.0	0.3927	8205	13726.900	0.02279	27454	2.7454E6	3.411E-3	0.8	2.3
47.000	300.0	2956.0	10000	20.0	5.155	138.000	235.2	600.0	0.3920	8205	14102.700	0.02279	28205	2.8205E6	3.411E-3	0.8	2.3
48.016	300.0	2934.9	10000	20.0	5.164	139.016	233.6	600.0	0.3893	8218	14360.700	0.02283	28721	2.8721E6	3.411E-3	0.8	2.3
49.000	300.0	2944.7	10000	20.0	5.177	140.000	234.3	600.0	0.3905	8239	14605.400	0.02288	29211	2.9211E6	3.411E-3	0.8	2.3
50.000	300.0	2957.8	10000	20.0	5.167	141.000	235.4	600.0	0.3923	8224	14984.300	0.02284	29969	2.9969E6	3.411E-3	0.8	2.4
50.996	300.0	2981.5	10000	20.0	5.167	141.996	237.3	600.0	0.3954	8223	15246.300	0.02284	30493	3.0493E6	3.411E-3	0.8	2.4
52.008	300.0	2976.0	10000	20.0	5.180	143.008	236.8	600.0	0.3947	8244	15610.700	0.02290	31221	3.1221E6	3.411E-3	0.9	2.4
52.996	300.0	2931.5	10000	20.0	5.165	143.996	233.3	600.1	0.3888	8220	15863.600	0.02283	31727	3.1727E6	3.411E-3	0.9	2.4
54.000	300.0	2934.1	10000	20.0	5.167	145.000	233.5	600.0	0.3892	8223	16115.200	0.02284	32230	3.2230E6	3.411E-3	0.9	2.4
55.000	300.0	2933.7	10000	20.0	5.168	146.000	233.5	600.0	0.3891	8225	16490.400	0.02285	32981	3.2981E6	3.411E-3	0.9	2.4
56.008	300.0	2941.4	10000	20.0	5.144	147.008	234.1	600.0	0.3901	8187	16743.100	0.02274	33486	3.3486E6	3.411E-3	0.9	2.5
57.000	300.0	2916.2	10000	20.0	5.169	148.000	232.1	600.0	0.3868	8226	17120.400	0.02285	34241	3.4241E6	3.411E-3	1.0	2.5
58.000	300.0	2965.2	10000	20.0	5.151	149.000	236.0	600.0	0.3933	8198	17370.000	0.02277	34740	3.4740E6	3.411E-3	1.0	2.5
59.000	300.0	2967.5	10000	20.0	5.178	150.000	236.1	600.0	0.3936	8241	17622.500	0.02289	35245	3.5245E6	3.411E-3	1.0	2.5
60.000	300.0	2941.2	10000	20.0	5.156	151.000	234.1	600.0	0.3901	8206	17998.400	0.02279	35997	3.5997E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0120	297.4	2927.7	10000	20.0	5.172	152.012	233.0	594.7	0.3918	8232	235.0200	0.02327	470.04	47004	3.411E-3	0.0	2.5
2.0080	291.3	2795.1	10000	20.0	5.200	153.008	222.4	582.7	0.3817	8276	593.5820	0.02438	1187.2	1.1872E5	3.411E-3	0.0	2.6
3.0080	287.3	2673.5	10000	20.0	5.226	154.008	212.8	574.7	0.3702	8318	830.1580	0.02519	1660.3	1.6603E5	3.411E-3	0.1	2.6
4.0080	281.2	2566.9	10000	20.0	5.296	155.008	204.3	562.3	0.3633	8429	1182.9000	0.02666	2365.8	2.3658E5	3.411E-3	0.1	2.6
5.0080	277.2	2419.6	10000	20.0	5.327	156.008	192.5	554.3	0.3474	8479	1406.0900	0.02759	2812.2	2.8122E5	3.411E-3	0.1	2.6
6.0080	273.0	2365.4	10000	20.0	5.324	157.008	188.2	546.1	0.3447	8474	1632.1500	0.02842	3264.3	3.2643E5	3.411E-3	0.1	2.6
7.0080	266.9	2205.1	10000	20.0	5.367	158.008	175.5	533.8	0.3287	8542	1971.2700	0.02998	3942.5	3.9425E5	3.411E-3	0.1	2.6
8.0080	262.8	2167.4	10000	20.0	5.372	159.008	172.5	525.7	0.3281	8550	2182.3999	0.03094	4364.8	4.3648E5	3.411E-3	0.1	2.7
9.0000	256.8	2056.9	10000	20.0	5.415	160.000	163.7	513.6	0.3187	8618	2501.6101	0.03268	5003.2	5.0032E5	3.411E-3	0.2	2.7
10.008	252.6	2005.8	10000	20.0	5.413	161.008	159.6	505.3	0.3159	8616	2714.6799	0.03374	5429.4	5.4294E5	3.411E-3	0.2	2.7
11.008	246.5	1957.6	10000	20.0	5.438	162.008	155.8	493.0	0.3160	8656	3022.1101	0.03561	6044.2	6.0442E5	3.411E-3	0.2	2.7
11.992	242.4	1876.2	10000	20.0	5.454	162.992	149.3	484.8	0.3079	8680	3221.4099	0.03693	6442.8	6.4428E5	3.411E-3	0.2	2.7
12.996	238.3	1825.0	10000	20.0	5.475	163.996	145.2	476.6	0.3047	8714	3421.7300	0.03836	6843.5	6.8435E5	3.411E-3	0.2	2.7
14.008	232.2	1732.8	10000	20.0	5.490	165.008	137.9	464.4	0.2969	8737	3709.5801	0.04051	7419.2	7.4192E5	3.411E-3	0.2	2.8
15.012	228.1	1687.1	10000	20.0	5.506	166.012	134.3	456.3	0.2942	8763	3897.1699	0.04209	7794.3	7.7943E5	3.411E-3	0.3	2.8
16.008	222.0	1593.2	10000	20.0	5.521	167.008	126.8	444.0	0.2856	8787	4178.7998	0.04458	8357.6	8.3576E5	3.411E-3	0.3	2.8
16.992	217.8	1566.9	10000	20.0	5.523	167.992	124.7	435.6	0.2862	8791	4360.3599	0.04632	8720.7	8.7207E5	3.411E-3	0.3	2.8
18.008	213.8	1492.0	10000	20.0	5.557	169.008	118.7	427.6	0.2777	8845	4535.3701	0.04838	9070.7	9.0707E5	3.411E-3	0.3	2.8
19.000	207.6	1435.4	10000	20.0	5.570	170.000	114.2	415.2	0.2751	8864	4798.0200	0.05142	9596.0	9.5960E5	3.411E-3	0.3	2.8
19.992	203.4	1395.6	10000	20.0	5.573	170.992	111.1	406.8	0.2730	8869	4973.1299	0.05360	9946.3	9.9463E5	3.411E-3	0.3	2.8
21.012	197.3	1323.6	10000	20.0	5.585	172.012	105.3	394.6	0.2669	8889	5218.1602	0.05710	10436	1.0436E6	3.411E-3	0.4	2.9
22.008	193.2	1271.9	10000	20.0	5.598	173.008	101.2	386.3	0.2620	8909	5379.8398	0.05970	10760	1.0760E6	3.411E-3	0.4	2.9
22.992	188.9	1231.3	10000	20.0	5.614	173.992	97.98	377.9	0.2593	8935	5542.2900	0.06256	11085	1.1085E6	3.411E-3	0.4	2.9
24.000	182.9	1157.3	10000	20.0	5.624	175.000	92.10	365.7	0.2518	8951	5767.1899	0.06692	11534	1.1534E6	3.411E-3	0.4	2.9
24.996	178.8	1124.6	10000	20.0	5.633	175.996	89.49	357.5	0.2503	8965	5917.1299	0.07014	11834	1.1834E6	3.411E-3	0.4	2.9
25.992	172.4	1048.5	10000	20.0	5.647	176.992	83.44	344.9	0.2420	8988	6143.1699	0.07558	12286	1.2286E6	3.411E-3	0.4	2.9
26.992	168.3	1017.5	10000	20.0	5.655	177.992	80.97	336.7	0.2405	9001	6279.5698	0.07941	12559	1.2559E6	3.411E-3	0.4	3.0
28.012	164.3	972.97	10000	20.0	5.667	179.012	77.43	328.5	0.2357	9019	6417.0601	0.08357	12834	1.2834E6	3.411E-3	0.5	3.0
29.000	157.9	907.60	10000	20.0	5.685	180.000	72.22	315.8	0.2287	9047	6623.4600	0.09071	13247	1.3247E6	3.411E-3	0.5	3.0
30.000	153.9	868.21	10000	20.0	5.687	181.000	69.09	307.7	0.2245	9052	6747.8799	0.09560	13496	1.3496E6	3.411E-3	0.5	3.0
30.996	149.8	836.82	10000	20.0	5.700	181.996	66.59	299.5	0.2223	9072	6942.0098	0.1011	13884	1.3884E6	3.411E-3	0.5	3.0
32.008	143.4	777.42	10000	20.0	5.709	183.008	61.87	286.9	0.2156	9087	7060.0298	0.1104	14120	1.4120E6	3.411E-3	0.5	3.1
33.008	139.2	742.96	10000	20.0	5.713	184.008	59.12	278.4	0.2124	9092	7178.5498	0.1173	14357	1.4357E6	3.411E-3	0.6	3.1
34.008	133.1	689.13	10000	20.0	5.723	185.008	54.84	266.1	0.2061	9108	7347.0601	0.1286	14694	1.4694E6	3.411E-3	0.6	3.1
35.008	128.8	646.10	10000	20.0	5.734	186.008	51.41	257.6	0.1996	9126	7459.1802	0.1375	14918	1.4918E6	3.411E-3	0.6	3.1
35.992	124.6	616.07	10000	20.0	5.741	186.992	49.03	249.1	0.1968	9136	7565.2500	0.1472	15131	1.5131E6	3.411E-3	0.6	3.1
36.992	118.5	565.10	10000	20.0	5.752	187.992	44.97	236.9	0.1898	9154	7714.8398	0.1631	15430	1.5430E6	3.411E-3	0.6	3.1
38.008	114.2	534.83	10000	20.0	5.755	189.008	42.56	228.4	0.1863	9159	7814.4800	0.1755	15629	1.5629E6	3.411E-3	0.6	3.2
39.008	109.8	500.61	10000	20.0	5.768	190.008	39.84	219.6	0.1814	9180	7913.9800	0.1903	15828	1.5828E6	3.411E-3	0.7	3.2
40.008	103.6	461.54	10000	20.0	5.774	191.008	36.73	207.2	0.1773	9190	8044.8198	0.2141	16090	1.6090E6	3.411E-3	0.7	3.2
40.992	99.35	425.14	10000	20.0	5.783	191.992	33.83	198.7	0.1703	9204	8132.2202	0.2331	16264	1.6264E6	3.411E-3	0.7	3.2
42.008	94.91	394.37	10000	20.0	5.791	193.008	31.38	189.8	0.1653	9217	8218.8896	0.2558	16438	1.6438E6	3.411E-3	0.7	3.2
43.008	88.71	356.21	10000	20.0	5.796	194.008	28.35	177.4	0.1598	9225	8332.2900	0.2930	16665	1.6665E6	3.411E-3	0.7	3.2
44.008	84.45	328.20	10000	20.0	5.798	195.008	26.12	168.9	0.1546	9228	8405.3398	0.3235	16811	1.6811E6	3.411E-3	0.7	3.3
45.008	79.96	298.48	10000	20.0	5.810	196.008	23.75	159.9	0.1485	9247	8479.6904	0.3615	16959	1.6959E6	3.411E-3	0.8	3.3
46.012	73.36	258.92	10000	20.0	5.812	197.012	20.60	146.7	0.1404	9250	8578.9004	0.4298	17158	1.7158E6	3.411E-3	0.8	3.3
46.992	69.04	235.42	10000	20.0	5.820	197.992	18.73	138.1	0.1357	9263	8641.1201	0.4858	17282	1.7282E6	3.411E-3	0.8	3.3
48.008	64.46	212.35	10000	20.0	5.820	199.008	16.90	128.9	0.1311	9263	8702.8398	0.5573	17406	1.7406E6	3.411E-3	0.8	3.3
49.000	59.79	187.18	10000	20.0	5.830	200.000	14.90	119.6	0.1246	9279	8758.1396	0.6490	17516	1.7516E6	3.411E-3	0.8	3.3
50.008	55.54	166.72	10000	20.0	5.835	201.008	13.27	111.1	0.1194	9287	8807.4805	0.7527	17615	1.7615E6	3.411E-3	0.8	3.4
51.008	50.96	145.10	10000	20.0	5.839	202.008	11.55	101.9	0.1133	9293	8856.7002	0.8947	17713	1.7713E6	3.411E-3	0.9	3.4
52.008	43.58	121.17	10000	20.0	5.844	203.008	9.643	87.15	0.1106	9302	8924.5996	1.225	17849	1.7849E6	3.411E-3	0.9	3.4
53.008	39.17	95.606	10000	20.0	5.850	204.008	7.608	78.34	0.09712	9310	8960.8604	1.517	17922	1.7922E6	3.411E-3	0.9	3.4
54.000	34.23	74.838	10000	20.0	5.850	205.000	5.955	68.47	0.08698	9311	8997.3096	1.986	17995	1.7995E6	3.411E-3	0.9	3.4
55.004	29.04	56.539	10000	20.0	5.855	206.004	4.499	58.07	0.07748	9319	9027.5098	2.763	18055	1.8055E6	3.411E-3	0.9	3.4
56.012	24.56	43.396	10000	20.0	5.857	207.012	3.453	49.12	0.07031	9322	9051.5801	3.864	18103	1.8103E6	3.411E-3	0.9	3.5
57.008	22.01	36.423	10000	20.0	5.857	208.008	2.898	44.02	0.06584	9322	9063.4404	4.810	18127	1.8127E6	3.411E-3	1.0	3.5
57.992	15.89	21.091	10000	20.0	5.858	208.992	1.678	31.77	0.05283	9324	9086.4502	9.237	18173	1.8173E6	3.411E-3	1.0	3.5
59.012	10.59	10.564	10000	20.0	5.860	210.012	0.8407	21.17	0.03971	9327	9097.8701	20.81	18196	1.8196E6	3.411E-3	1.0	3.5
59.992	4.555	1.1652	10000	20.0	5.863	210.992	0.09273	9.109	0.01018	9331	9105.4600	112.4	18211	1.8211E6	3.411E-3	1.0	3.5

